Technology Process of C39H57F3N2O5
There total 6 articles about C39H57F3N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
chloroform;
at 20 ℃;
for 24h;
DOI:10.1016/j.tet.2010.11.046
- Guidance literature:
-
Multi-step reaction with 5 steps
1: ethanol; iron; ammonium chloride / 5 h / Reflux
2: triethylamine / chloroform / 0 - 20 °C
3: nitric acid; acetic acid / chloroform / 0.25 h / 0 °C
4: tin(II) chloride hydrate / ethyl acetate / 2 h / Reflux
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform / 24 h / 20 °C
With
tin(II) chloride hydrate; ethanol; nitric acid; iron; ammonium chloride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
chloroform; ethyl acetate;
DOI:10.1016/j.tet.2010.11.046
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tin(II) chloride hydrate / ethyl acetate / 2 h / Reflux
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform / 24 h / 20 °C
With
tin(II) chloride hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
chloroform; ethyl acetate;
DOI:10.1016/j.tet.2010.11.046