9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

Base Information

Chemical Name:9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene
CAS No.:1246081-80-0
Molecular Formula:C₇₆H₇₀O₉
Molecular Weight:1127.39
Hs Code.:

Synonyms:9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

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Chemical Property of 9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

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Technology Process of 9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

There total 4 articles about 9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1246081-83-3
7-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-22-((2S)-2-methylbutoxy)-3-oxahexacyclo[7.6.6.2(5,8).0(1,5).0(10,15).0(16,21)]tricosa-6,10,12,14,16,18,20,22-octaene

: 1246081-80-0
9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

Guidance literature:: In benzene; at 60 ℃;
DOI:10.1002/asia.201000159

Reference yield: 40.0%

: 24463-19-2
anthracenylmethyl chloride

: 1246081-76-4
3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)-benzyl alcohol

: 1246081-80-0
9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

Guidance literature:: With tetrabutylammomium bromide; potassium hydroxide; In N,N-dimethyl-formamide; at 60 ℃; for 48h; Inert atmosphere;
DOI:10.1002/asia.201000159

Reference yield:

: 184219-30-5
C₄₉H₄₃ClO₆

: 1246081-80-0
9-[(3-{3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyloxy}-5-((2S)-2-methylbutoxy)benzyloxy)methyl]anthracene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone

2: tetrabutylammomium bromide; potassium hydroxide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

3: tetrabutylammomium bromide; potassium hydroxide / N,N-dimethyl-formamide / 48 h / 60 °C / Inert atmosphere

With tetrabutylammomium bromide; potassium carbonate; potassium hydroxide; In N,N-dimethyl-formamide; acetone;
DOI:10.1002/asia.201000159