3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

Base Information

Chemical Name:3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol
CAS No.:278610-81-4
Molecular Formula:C₅₆H₅₀O₉
Molecular Weight:867.008
Hs Code.:

Synonyms:3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

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Chemical Property of 3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

Chemical Property:

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Technology Process of 3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

There total 8 articles about 3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 129536-41-0
3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyl bromide

: 278610-81-4
3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/ol0608956

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 278610-81-4
3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

Guidance literature:: Multi-step reaction with 6 steps

1: 4-(dimethylamino)pyridine; triethylamine / tetrahydrofuran / 3 h / 20 °C

2: lithium bromide / tetrahydrofuran / Heating

3: 23 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

4: (dimethylamino)pyridine; triethylamine / tetrahydrofuran / 3 h / 20 °C

5: lithium bromide / tetrahydrofuran / Heating

6: 84 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

With dmap; 18-crown-6 ether; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran;
DOI:10.1021/ol0608956

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 278610-81-4
3-[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-benzyloxy]-5-hydroxymethyl-phenol

Guidance literature:: Multi-step reaction with 4 steps

1: 23 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

2: (dimethylamino)pyridine; triethylamine / tetrahydrofuran / 3 h / 20 °C

3: lithium bromide / tetrahydrofuran / Heating

4: 84 percent / K₂CO₃; 18-crown-6 / tetrahydrofuran / 12 h / Heating

With dmap; 18-crown-6 ether; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran;
DOI:10.1021/ol0608956