4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

Base Information

Chemical Name:4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol
CAS No.:127679-95-2
Molecular Formula:C₂₆H₂₆Br₂Cl₂O₃
Molecular Weight:617.205
Hs Code.:

Synonyms:4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

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Chemical Property of 4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

Chemical Property:

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Technology Process of 4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

There total 3 articles about 4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 127679-91-8
4-Tert-butyl-2,6-bis<(5-chloro-3-hydroxymethyl-2-hydroxyphenyl)methyl>phenol

: 127679-95-2
4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

Guidance literature:: With hydrogen bromide; In acetic acid; for 35h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85448-X

Reference yield:

: 2203-14-7
4-tert-butyl-2,5-bis(hydroxymethyl)phenol

: 127679-95-2
4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / conc. H₂SO₄ / 0.5 h / 80 - 90 °C

2: 75 percent / aq. NaOH / 24 h / 50 °C

3: 58 percent / HBr / acetic acid / 35 h / Ambient temperature

With hydrogen bromide; sulfuric acid; In sodium hydroxide; acetic acid;
DOI:10.1016/S0040-4020(01)85448-X

Reference yield:

: 127679-79-2
4-tert-Butyl-2,6-bis<(5-chloro-2-hydroxyphenyl)methyl>phenol

: 127679-95-2
4-Tert-butyl-2,6-bis<(3-bromomethyl-5-chloro-2-hydroxyphenyl)methyl>phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / aq. NaOH / 24 h / 50 °C

2: 58 percent / HBr / acetic acid / 35 h / Ambient temperature

With hydrogen bromide; In sodium hydroxide; acetic acid;
DOI:10.1016/S0040-4020(01)85448-X