1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

Base Information

Chemical Name:1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene
CAS No.:443643-12-7
Molecular Formula:C₂₂H₁₈N₈O₂
Molecular Weight:426.437
Hs Code.:

Synonyms:1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

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Chemical Property of 1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

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Technology Process of 1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

There total 4 articles about 1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 443643-19-4
1,4-bis(acylpyridin-2'-ylamidrazone)-2,5-dimethoxybenzene

: 443643-12-7
1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

Guidance literature:: With ethylene glycol; Heating;
DOI:10.1039/b108728m

Reference yield:

: 21004-11-5
2,5-dimethoxyterephthalic acid

: 443643-12-7
1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅ / Heating

2: 67 percent / Na₂CO₃ / tetrahydrofuran / 24 h / 0 °C

3: 54 percent / ethylene glycol / Heating

With phosphorus pentachloride; sodium carbonate; ethylene glycol; In tetrahydrofuran;
DOI:10.1039/b108728m

Reference yield:

: 173267-23-7
diethyl-2,5-dimethoxy-1,4-benzenedicarboxylate

: 443643-12-7
1,4-bis(5'-(pyridin-2-yl)-1'H-1',2',4'-triazol-3'-yl)-2,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / KOH / ethane-1,2-diol / 100 °C

2: PCl₅ / Heating

3: 67 percent / Na₂CO₃ / tetrahydrofuran / 24 h / 0 °C

4: 54 percent / ethylene glycol / Heating

With potassium hydroxide; phosphorus pentachloride; sodium carbonate; ethylene glycol; In tetrahydrofuran; ethylene glycol;
DOI:10.1039/b108728m