[phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester

Base Information

Chemical Name:[phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester
CAS No.:1075239-88-1
Molecular Formula:C₃₁H₂₆IN₃O₇
Molecular Weight:679.468
Hs Code.:

Synonyms:[phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester

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Chemical Property of [phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester

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Technology Process of [phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester

There total 1 articles about [phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1075239-91-6
[phthaloyl-(1-carbobenzyloxy-D-tryptophanyl)]-L-alanine methyl ester

: 1075239-88-1
[phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester

Guidance literature:: [phthaloyl-(1-carbobenzyloxy-D-tryptophanyl)]-L-alanine methyl ester; With mercury(II) trifluoroacetate; In dichloromethane; for 0.583333h; Inert atmosphere;

With iodine; for 0.666667h;
DOI:10.1021/ol802155n

Reference yield: 64.0%

: 1075239-88-1
[phthaloyl-(1-carbobenzyloxy-2-iodo-D-tryptophanyl)]-L-alanine methyl ester

: 1075239-91-6
[phthaloyl-(1-carbobenzyloxy-D-tryptophanyl)]-L-alanine methyl ester

: 1075239-92-7
(1S,3R)-9-carbobenzyloxy-3-phthalimido-1-(1-methoxycarbonyl-ethyl)-2-oxo-1,2,3,4-tetrahydro-pyrido[2,3-b]indole

Guidance literature:: With potassium phosphate; copper(l) iodide; trans-N,N'-dimethylcyclohexane-1,2-diamine; In toluene; at 110 ℃; for 17h; Inert atmosphere;
DOI:10.1021/ol802155n