(E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester

Base Information

Chemical Name:(E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester
CAS No.:745021-33-4
Molecular Formula:C₁₅H₂₀O₂
Molecular Weight:232.323
Hs Code.:

Synonyms:(E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester

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Technology Process of (E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester

There total 2 articles about (E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 56453-88-4
(E)-3-(1-cyclohexen-1-yl)-2-propenoic acid

: 745021-32-3
(Z)-(S)-Hexa-3,5-dien-2-ol

: 745021-33-4
(E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester

Guidance literature:: With dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1016/j.bmcl.2004.05.047

Reference yield:

: tert-Butyl-dimethyl-((Z)-(S)-1-methyl-penta-2,4-dienyloxy)-silane

: 745021-33-4
(E)-3-Cyclohex-1-enyl-acrylic acid (Z)-(S)-1-methyl-penta-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / methanol

2: 75 percent / EDCI; DMAP; TEMPO / CH₂Cl₂

With dmap; 2,2,6,6-tetramethyl-piperidine-N-oxyl; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2004.05.047