Technology Process of C36H34O7
There total 7 articles about C36H34O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/ol3016463
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Montmorillonite K-10 clay / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
1.2: 13.5 h / 20 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere
3.1: AD-mix-α; methanesulfonamide / dichloromethane; water; tert-butyl alcohol / 72 h / 0 - 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere
With
methanesulfonamide; AD-mix-α; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
1.1: Friedel Crafts alkylation / 1.2: Friedel Crafts alkylation;
DOI:10.1021/ol3016463
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / toluene / 2.5 h / -78 - 20 °C / Inert atmosphere
2.1: Montmorillonite K-10 clay / dichloromethane / 0.25 h / 20 °C / Inert atmosphere
2.2: 13.5 h / 20 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere
4.1: AD-mix-α; methanesulfonamide / dichloromethane; water; tert-butyl alcohol / 72 h / 0 - 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere
With
methanesulfonamide; AD-mix-α; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol;
2.1: Friedel Crafts alkylation / 2.2: Friedel Crafts alkylation;
DOI:10.1021/ol3016463