N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide
CAS No.:1342795-39-4
Molecular Formula:C₁₉H₁₈ClNO₂S
Molecular Weight:359.876
Hs Code.:

Synonyms:N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Suppliers and Price of N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

There total 7 articles about N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 637-87-6
1-Chloro-4-iodobenzene

: 133886-40-5
N-tosyl-N-allylpropargylamine

: 1342795-39-4
N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201704401

Reference yield: 58.0%

: 1239189-22-0
N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

: 106-95-6
allyl bromide

: 1342795-39-4
N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

allyl bromide; In N,N-dimethyl-formamide; mineral oil; Inert atmosphere;
DOI:10.1002/chem.201101745

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1342795-39-4
N-allyl-N-(3-(4-chlorophenyl)prop-2-yn-1-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 5 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / Sealed tube; Reflux

3: triethylamine; trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1002/chem.201704401