{C₅(CH₃)5Ir(CH₃)C₈H₆S}⁽¹⁺⁾*(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₆S}BF₄

Base Information

• Chemical Name: {C₅(CH₃)5Ir(CH₃)C₈H₆S}⁽¹⁺⁾*(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₆S}BF₄
• CAS No.: 114032-65-4
• Molecular Formula: BF₄*C₁₉H₂₄IrS
• Molecular Weight: 563.49
• Mol file: 114032-65-4.mol

Synonyms:{C₅(CH₃)5Ir(CH₃)C₈H₆S}⁽¹⁺⁾*(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₆S}BF₄

Chemical Property of {C₅(CH₃)5Ir(CH₃)C₈H₆S}⁽¹⁺⁾*(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₆S}BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of {C₅(CH₃)5Ir(CH₃)C₈H₆S}⁽¹⁺⁾*(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₆S}BF₄

There total 1 articles about {C₅(CH₃)5Ir(CH₃)C₈H₆S}⁽¹⁺⁾*(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₆S}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

sodium tetrahydroborate (16940-66-2) + {C5(CH3)5Ir(CH3)C8H5S}(2+)*2(BF4)(1-)={C5(CH3)5Ir(CH3)C8H5S}(BF4)2 (114032-45-0) → sodium tetrafluoroborate (13755-29-8) + {C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4 (114032-65-4) + {C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4 (114032-63-2) + {C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4 (114057-30-6) + {C5(CH3)5Ir(CH3)C8H6S}(1+)*(BF4)(1-)={C5(CH3)5Ir(CH3)C8H6S}BF4 (114032-61-0)

Guidance literature:

In dichloromethane; water; H2O and CH2Cl2 were purged with N2 for 5 min. To this stirred soln. was added (C5(CH3)5Ir(2-MeBT))(BF4)2 and then NaBH4.; After 5 min the layers were sepd., and the water layer was extd. with CH2Cl2. The combined CH2Cl2 extracts were dried over Na2SO4 and filtered. Product was pptd. by addn. of Et2O. elem. anal.; ratio of isomers: 60:23:9:8;

upstream raw materials:

sodium tetrahydroborate

{C₅(CH₃)5Ir(CH₃)C₈H₅S}⁽²⁺⁾*2(BF₄)^(1-)={C₅(CH₃)5Ir(CH₃)C₈H₅S}(BF₄)2