Cyclohexanecarboxamide, 1-amino-2-methyl-, (1S-trans)- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxamide, 1-amino-2-methyl-, (1S-trans)- (9CI)
CAS No.:184035-02-7
Molecular Formula:C8H16 N2 O
Molecular Weight:156.228
Hs Code.:
Mol file:184035-02-7.mol

Synonyms:Cyclohexanecarboxamide,1-amino-2-methyl-, (1S-trans)- (9CI)

Suppliers and Price of Cyclohexanecarboxamide, 1-amino-2-methyl-, (1S-trans)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Cyclohexanecarboxamide, 1-amino-2-methyl-, (1S-trans)- (9CI)

Chemical Property:

PSA：69.11000
LogP:1.77990

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxamide, 1-amino-2-methyl-, (1S-trans)- (9CI)

There total 6 articles about Cyclohexanecarboxamide, 1-amino-2-methyl-, (1S-trans)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 184035-13-0
(1S,2S)-2-Methyl-1-((R)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: 184035-02-7
(1S,2S)-1-Amino-2-methyl-cyclohexanecarboxylic acid amide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 45 ℃; for 24h; under 3750.3 Torr;
DOI:10.1002/jlac.199619961126

Reference yield:

: 184034-98-8
(1S,2S)-2-Methyl-1-((S)-1-phenyl-ethylamino)-cyclohexanecarboxylic acid amide

: 184035-02-7
(1S,2S)-1-Amino-2-methyl-cyclohexanecarboxylic acid amide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 45 ℃; for 24h; under 3750.3 Torr;
DOI:10.1002/jlac.199619961126

Reference yield:

: 828291-16-3
E/Z-<2(RS)>-2-Methyl-N-(R-α-methylbenzyl)-cyclohexaneimine

: 184035-02-7
(1S,2S)-1-Amino-2-methyl-cyclohexanecarboxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 3 h / 0 °C

2: conc. H₂SO₄ / hexane / 102 h

3: 99 percent / H₂ / 10percent Pd/C / ethanol / 24 h / 45 °C / 3750.3 Torr

With sulfuric acid; hydrogen; palladium on activated charcoal; In methanol; ethanol; hexane;
DOI:10.1002/jlac.199619961126