C₃₁H₄₂O₄Si₂

Base Information

Chemical Name:C₃₁H₄₂O₄Si₂
CAS No.:1334173-62-4
Molecular Formula:C₃₁H₄₂O₄Si₂
Molecular Weight:534.843
Hs Code.:

C<sub>31</sub>H<sub>42</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₁H₄₂O₄Si₂

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Chemical Property of C₃₁H₄₂O₄Si₂

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Technology Process of C₃₁H₄₂O₄Si₂

There total 4 articles about C₃₁H₄₂O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 201230-82-2
carbon monoxide

: C₃₀H₄₂O₃SSi

: 1334173-62-4
C₃₁H₄₂O₄Si₂

Guidance literature:: C₃₀H₄₂O₃SSi; With dicobalt octacarbonyl; In toluene; at 20 ℃; for 1h; Inert atmosphere;

carbon monoxide; In toluene; at 100 ℃; for 15h; stereoselective reaction;
DOI:10.1002/anie.201103550

Reference yield:

: 1334173-55-5
C₂₈H₃₈O₃Si

: 1334173-62-4
C₃₁H₄₂O₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

2.1: dicobalt octacarbonyl / toluene / 1 h / 20 °C / Inert atmosphere

2.2: 15 h / 100 °C

With dmap; dicobalt octacarbonyl; triethylamine; In dichloromethane; toluene; 2.1: Pauson-Khand reaction / 2.2: Pauson-Khand reaction;
DOI:10.1002/anie.201103550

Reference yield:

: 1334173-59-9
C₂₈H₃₄O₃Si

: 1334173-62-4
C₃₁H₄₂O₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

3.1: dicobalt octacarbonyl / toluene / 1 h / 20 °C / Inert atmosphere

3.2: 15 h / 100 °C

With dmap; lithium borohydride; dicobalt octacarbonyl; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 3.1: Pauson-Khand reaction / 3.2: Pauson-Khand reaction;
DOI:10.1002/anie.201103550