((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

Base Information

Chemical Name:((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane
CAS No.:132585-91-2
Molecular Formula:C₁₇H₂₇N₃O₂SSi
Molecular Weight:365.572
Hs Code.:

Synonyms:((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

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Chemical Property of ((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

Chemical Property:

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Technology Process of ((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

There total 5 articles about ((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid (2R,3R,5R)-2-(tert-butyl-dimethyl-silanyloxymethyl)-5-phenylsulfanyl-tetrahydro-furan-3-yl ester

: 132585-91-2
((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; Yield given;
DOI:10.1016/S0040-4039(00)74336-X

Reference yield:

: (2S,3R,5R)-3-Hydroxy-5-phenylsulfanyl-tetrahydro-furan-2-carbaldehyde

: 132585-91-2
((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄

2: 88 percent / Et₃N / DMAP

3: pyridine

4: sodium azide / dimethylformamide / 100 °C

With pyridine; sodium tetrahydroborate; sodium azide; triethylamine; dmap; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)74336-X

Reference yield:

: 134614-93-0
Phenyl 2-deoxy-1-thio-α-D-threo-pentofuranoside

: 132585-91-2
((2S,3S,5R)-3-Azido-5-phenylsulfanyl-tetrahydro-furan-2-ylmethoxy)-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N / DMAP

2: pyridine

3: sodium azide / dimethylformamide / 100 °C

With pyridine; sodium azide; triethylamine; dmap; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)74336-X