Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI)

Base Information

Chemical Name:Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI)
CAS No.:183990-21-8
Molecular Formula:C₉H₁₈ClNO₂
Molecular Weight:207.7
Hs Code.:
Mol file:183990-21-8.mol

Synonyms:Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI)

Suppliers and Price of Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI)

Chemical Property:

PSA：38.33000
LogP:2.91940

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI)

There total 1 articles about Carbamic acid, [1-(chloromethyl)propyl]-, 1,1-dimethylethyl ester, (R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 763862-66-4
(R)-1-Chloromethyl-propylamine

: 183990-21-8
((R)-1-Chloromethyl-propyl)-carbamic acid tert-butyl ester

Guidance literature:: With sodium carbonate; triethylamine; In methanol; at 65 ℃; for 1h; Yield given;
DOI:10.1016/0957-4166(96)00382-5

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 183990-21-8
((R)-1-Chloromethyl-propyl)-carbamic acid tert-butyl ester

: 183990-48-9,557091-78-8
(3R)-3-(tert-butoxycarbonylamino)pentanoic acid

Guidance literature:: With n-butyllithium; LiC₁₀H₇; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 3 h, 2.) THF, hexane, from -78 to 20 deg C, overnight;
DOI:10.1016/0957-4166(96)00382-5

Reference yield:

: 538-75-0
dicyclohexyl-carbodiimide

: 183990-21-8
((R)-1-Chloromethyl-propyl)-carbamic acid tert-butyl ester

: (R)-1-Cyclohexyl-6-[(E)-cyclohexylimino]-4-ethyl-tetrahydro-pyrimidin-2-one

Guidance literature:: With n-butyllithium; LiC₁₀H₇; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 3 h, 2.) THF, hexane, from -78 to 20 deg C, overnight;
DOI:10.1016/0957-4166(96)00382-5