C₂₆H₂₁F₃N₂O₂

Base Information

Chemical Name:C₂₆H₂₁F₃N₂O₂
CAS No.:1329990-89-7
Molecular Formula:C₂₆H₂₁F₃N₂O₂
Molecular Weight:450.46
Hs Code.:

C<sub>26</sub>H<sub>21</sub>F<sub>3</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₆H₂₁F₃N₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₁F₃N₂O₂

Chemical Property:

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Technology Process of C₂₆H₂₁F₃N₂O₂

There total 8 articles about C₂₆H₂₁F₃N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329990-88-6
C₂₆H₂₁F₃N₂O₂

: 1329990-89-7
C₂₆H₂₁F₃N₂O₂

: 1329990-90-0
C₂₆H₂₁F₃N₂O₂

Guidance literature:: With Chiracel OD; In water; acetonitrile; trifluoroacetic acid; Resolution of racemate;

Reference yield:

: 121-17-5
2-chloro-3-nitro-5-trifluoromethylbenzene

: 1329990-89-7
C₂₆H₂₁F₃N₂O₂

: 1329990-90-0
C₂₆H₂₁F₃N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / N,N-dimethyl-formamide / 1 h / 100 °C

2: triethylamine; formic acid / palladium 10% on activated carbon / ethanol / 2 h / Inert atmosphere

3: N,N-dimethyl-formamide / 1 h / 170 °C / Microwaves

4: lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 20 °C

5: pyridine; copper diacetate / dichloromethane / 4 h / 20 °C

6: caesium carbonate / tri-tert-butyl phosphine; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere

7: Chiracel OD / trifluoroacetic acid; acetonitrile; water / Resolution of racemate

With pyridine; formic acid; copper diacetate; caesium carbonate; triethylamine; lithium hexamethyldisilazane; bis(tri-t-butylphosphine)palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; trifluoroacetic acid;

Reference yield:

: 1074-16-4
2-bromophenylethyl alcohol

: 1329990-89-7
C₂₆H₂₁F₃N₂O₂

: 1329990-90-0
C₂₆H₂₁F₃N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1: 1H-imidazole; triphenylphosphine; iodine / diethyl ether; acetonitrile / 16 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

3: N,N-dimethyl-formamide / 1 h / 170 °C / Microwaves

4: lithium hexamethyldisilazane / tetrahydrofuran / 0.75 h / 20 °C

5: pyridine; copper diacetate / dichloromethane / 4 h / 20 °C

6: caesium carbonate / tri-tert-butyl phosphine; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 24 h / 80 °C / Inert atmosphere

7: Chiracel OD / trifluoroacetic acid; acetonitrile; water / Resolution of racemate

With pyridine; 1H-imidazole; iodine; copper diacetate; potassium carbonate; caesium carbonate; triphenylphosphine; lithium hexamethyldisilazane; bis(tri-t-butylphosphine)palladium⁽⁰⁾; tri-tert-butyl phosphine; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; trifluoroacetic acid;