diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

Base Information

Chemical Name:diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate
CAS No.:1192717-55-7
Molecular Formula:C₂₀H₂₅NO₄S
Molecular Weight:375.489
Hs Code.:

Synonyms:diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

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Chemical Property of diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

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Technology Process of diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

There total 3 articles about diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 542-81-4
sulfure de methyle et de 2-chloroethyle

: 3651-13-6
5-methyl-3-phenyl-1H-pyrrole-2,4-dicarboxylic acid diethyl ester

: 1192717-55-7
diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

Guidance literature:: 5-methyl-3-phenyl-1H-pyrrole-2,4-dicarboxylic acid diethyl ester; With potassium tert-butylate; In dimethyl sulfoxide; at 10 - 20 ℃;

sulfure de methyle et de 2-chloroethyle; In dimethyl sulfoxide; at 10 - 20 ℃;

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 1192717-55-7
diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; sodium nitrite / water / 0 - 20 °C

2.1: sodium acetate; zinc / acetic acid / 60 - 75 °C

3.1: potassium tert-butylate / dimethyl sulfoxide / 10 - 20 °C

3.2: 10 - 20 °C

With potassium tert-butylate; sodium acetate; acetic acid; zinc; sodium nitrite; In water; acetic acid; dimethyl sulfoxide;

Reference yield:

: 60317-41-1
ethyl 2-(hydroxyimino)-3-oxo-3-phenylpropanoate

: 1192717-55-7
diethyl 5-methyl-1-(2-methylsulfanylethyl)-3-phenyl-1H-pyrrole-2,4-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate; zinc / acetic acid / 60 - 75 °C

2.1: potassium tert-butylate / dimethyl sulfoxide / 10 - 20 °C

2.2: 10 - 20 °C

With potassium tert-butylate; sodium acetate; zinc; In acetic acid; dimethyl sulfoxide;