ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Base Information

Chemical Name:ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate
CAS No.:250601-74-2
Molecular Formula:C₃₂H₃₄N₂O₅
Molecular Weight:526.632
Hs Code.:

Synonyms:ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

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Technology Process of ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

There total 6 articles about ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 4248-25-3
ethyl 6-oxo-6-phenylhexanoate

: 250602-87-0
3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyamine

: 250601-74-2
ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Guidance literature:: With sodium chloride; sodium acetate; acetic acid; In ethanol; water;

Reference yield: 58.0%

: 4248-25-3
ethyl 6-oxo-6-phenylhexanoate

: 250602-87-0
3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyamine

: 250601-74-2
ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Guidance literature:: With sodium acetate; acetic acid; In ethanol; for 12h; Heating;
DOI:10.1248/cpb.51.138

Reference yield:

: 159017-85-3
3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzaldehyde

: 250601-74-2
ethyl (E)-6-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-6-phenylhexanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / sodium borohydride / methanol; tetrahydrofuran / 0.5 h / 20 °C

2: 84 percent / thionyl chloride / toluene / 0.5 h / 20 °C

3: 90 percent / K₂CO₃ / dimethylformamide / 20 h / 20 °C

4: 97 percent / hydrazine monohydrate / ethanol; tetrahydrofuran / 3 h / Heating

5: 58 percent / acetic acid; sodium acetate / ethanol / 12 h / Heating

With sodium tetrahydroborate; thionyl chloride; sodium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1248/cpb.51.138