2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

Base Information

Chemical Name:2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone
CAS No.:83520-24-5
Molecular Formula:C₂₉H₂₁Cl₂N₅O₄
Molecular Weight:574.423
Hs Code.:

Synonyms:2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

Suppliers and Price of 2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

There total 6 articles about 2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83520-08-5
2-Benzyloxycarbonylamino-N-[4-chloro-2-(2-chloro-benzoyl)-phenyl]-acetimidic acid ethyl ester

: 83520-24-5
2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / NH₂NH₂*H₂O, AcOH / ethanol / 2 h / Heating

2: HMPA / acetonitrile / 4 h / 0 °C

3: 25 percent / AcOH / 5 h / Heating

4: 30percent HBr-AcOH / 1 h / Ambient temperature

5: benzene; dimethylformamide / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; hydrogen bromide; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1021/jm00354a015

Reference yield:

: 64194-96-3
3-amino-2-<<(benzyloxycarbonyl)amino>methyl>-6-chloro-4-(2-chlorophenyl)-3,4-dihydro-4-hydroxyquinazoline

: 83520-24-5
2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

Guidance literature:: Multi-step reaction with 4 steps

1: HMPA / acetonitrile / 4 h / 0 °C

2: 25 percent / AcOH / 5 h / Heating

3: 30percent HBr-AcOH / 1 h / Ambient temperature

4: benzene; dimethylformamide / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; hydrogen bromide; acetic acid; In N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1021/jm00354a015

Reference yield:

: 83520-18-7
2',5-dichloro-2-<3-<<(benzyloxycarbonyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

: 83520-24-5
2',5-dichloro-2-<3-<<(phthaloylglycyl)amino>methyl>-5-cyclopropyl-4H-1,2,4-triazol-4-yl>benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 30percent HBr-AcOH / 1 h / Ambient temperature

2: benzene; dimethylformamide / Ambient temperature

With hydrogen bromide; acetic acid; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00354a015