Technology Process of C17H22BFO6
There total 8 articles about C17H22BFO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; potassium acetate;
In
1,4-dioxane;
at 95 ℃;
for 16h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.12.096
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; calcium carbonate / 1,4-dioxane / 16 h / 100 °C
2: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C
3: pyridinium p-toluenesulfonate / toluene / 16 h / 138 °C
4: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / 1,4-dioxane / 16 h / 95 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; water; potassium acetate; pyridinium p-toluenesulfonate; pyridinium chlorochromate; calcium carbonate;
In
1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2011.12.096
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C
2: pyridinium p-toluenesulfonate / toluene / 16 h / 138 °C
3: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / 1,4-dioxane / 16 h / 95 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium acetate; pyridinium p-toluenesulfonate; pyridinium chlorochromate;
In
1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2011.12.096
