O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine

Base Information

• Chemical Name: O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine
• CAS No.: 220645-39-6
• Molecular Formula: C₁₅H₂₃NO₂
• Molecular Weight: 249.353
• Mol file: 220645-39-6.mol

Synonyms:O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine

Chemical Property of O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine

There total 1 articles about O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

tert-Octylamine (107-45-9) + dibenzoyl peroxide (94-36-0) → O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine (220645-39-6)

Guidance literature:

With dipotassium hydrogenphosphate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1021/jo051999h

Reference yield: 82.0%

triphenylboroxine (3262-89-3) + O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine (220645-39-6) → N-(2,4,4-trimethylpentan-2-yl)aniline

Guidance literature:

triphenylboroxine; With potassium carbonate; In 1,4-dioxane; at 130 ℃; for 24h; Inert atmosphere;

O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine; In 1,4-dioxane; Inert atmosphere;

DOI:10.1021/ol301912a

Reference yield: 38.0%

p-tolylsulfinyl amide (6873-55-8) + O-benzoyl-N-(1,1,3,3-tetramethyl)butylhydroxylamine (220645-39-6) → 4-methyl-N-(2,4,4-trimethylpentan-2-yl)benzenesulfinamide

Guidance literature:

With triphenylphosphine; copper(ll) bromide; In 1,2-dichloro-ethane; at 60 ℃; for 12h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.201810548

upstream raw materials:

tert-Octylamine

dibenzoyl peroxide