Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

Base Information

Chemical Name:Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester
CAS No.:872130-29-5
Molecular Formula:C₂₈H₃₃O₇P
Molecular Weight:512.54
Hs Code.:

Synonyms:Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

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Technology Process of Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

There total 4 articles about Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 82130-78-7
(S)-2-benzyloxy-3-(5,5-dimethyl-1,3-dioxan-2-yl)propan-1-ol

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 872130-29-5
Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 5h;
DOI:10.1039/b511661a

Reference yield:

: (S)-3-benzyloxy-4-hydroxybutanal

: 872130-29-5
Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / TMSCl / CH₂Cl₂ / 5 h / 0 °C

2: 51 percent / imidazole / CH₂Cl₂ / 5 h / 0 - 20 °C

With 1H-imidazole; chloro-trimethyl-silane; In dichloromethane;
DOI:10.1039/b511661a

Reference yield:

: 101999-38-6,114784-20-2,121961-93-1,82130-75-4
(S)-4-benzyloxy-dihydrofuran-2(3H)-one

: 872130-29-5
Phosphoric acid (S)-2-benzyloxy-3-(5,5-dimethyl-[1,3]dioxan-2-yl)-propyl ester diphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / DIBAL-H / CH₂Cl₂ / -78 °C

2: 47 percent / TMSCl / CH₂Cl₂ / 5 h / 0 °C

3: 51 percent / imidazole / CH₂Cl₂ / 5 h / 0 - 20 °C

With 1H-imidazole; chloro-trimethyl-silane; diisobutylaluminium hydride; In dichloromethane;
DOI:10.1039/b511661a