3-isobutoxy-2-methylbenzyl amine

Base Information

Chemical Name:3-isobutoxy-2-methylbenzyl amine
CAS No.:467252-14-8
Molecular Formula:C₁₂H₁₉NO
Molecular Weight:193.289
Hs Code.:

Synonyms:3-isobutoxy-2-methylbenzyl amine

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Chemical Property of 3-isobutoxy-2-methylbenzyl amine

Chemical Property:

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Technology Process of 3-isobutoxy-2-methylbenzyl amine

There total 5 articles about 3-isobutoxy-2-methylbenzyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1-azidomethyl-3-isobutoxy-2-methyl-benzene

: 467252-14-8
3-isobutoxy-2-methylbenzyl amine

Guidance literature:: With thiophenol; triethylamine; tin(ll) chloride;
DOI:10.1021/jm0208673

Reference yield:

: 55289-05-9
methyl 3-hydroxy-2-methylbenzoate

: 467252-14-8
3-isobutoxy-2-methylbenzyl amine

Guidance literature:: Multi-step reaction with 5 steps

1: 58 percent / K₂CO₃ / acetonitrile / Heating

2: 98 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3: 100 percent / SOCl₂ / CH₂Cl₂ / 0.5 h / 20 °C

4: IR₄₀₀ N₃ ion exchange resin

5: 76 percent / SnCl₂; PhSH; Et₃N

With lithium aluminium tetrahydride; thionyl chloride; IR₄₀₀ N₃ ion exchange resin; potassium carbonate; thiophenol; triethylamine; tin(ll) chloride; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm0208673

Reference yield:

: 339354-79-9
3-isobutoxy-2-methylbenzyl alcohol

: 467252-14-8
3-isobutoxy-2-methylbenzyl amine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / SOCl₂ / CH₂Cl₂ / 0.5 h / 20 °C

2: IR₄₀₀ N₃ ion exchange resin

3: 76 percent / SnCl₂; PhSH; Et₃N

With thionyl chloride; IR₄₀₀ N₃ ion exchange resin; thiophenol; triethylamine; tin(ll) chloride; In dichloromethane;
DOI:10.1021/jm0208673