4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione

Base Information

• Chemical Name: 4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione
• CAS No.: 160409-44-9
• Molecular Formula: C₃₉H₄₆O₂S₅Si₂
• Molecular Weight: 763.294

Synonyms:4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione

Chemical Property of 4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione

Chemical Property:

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Technology Process of 4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione

There total 1 articles about 4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4,5-bis[(2'-hydroxyethyl)thio]1,3-dithiole-2-thione (128258-71-9) + tert-butylchlorodiphenylsilane (58479-61-1) → 4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione (160409-44-9)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1055/s-1994-25606

Reference yield: 100.0%

4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione (160409-44-9) → 4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one (160409-45-0)

Guidance literature:

With mercury(II) diacetate; In chloroform; acetic acid; at 20 ℃; for 16h;

DOI:10.1055/s-1994-25606

Reference yield: 73.0%

4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione (160409-44-9) + 3-(5-methylsulfanyl-2-oxo-1,3-dithiol-4-ylsulfanyl)propanenitrile (160624-09-9) → 2-(2-Cyanoethylthio)-3-methylthio-6,7-bis[2-(tert-butyldiphenylsilyloxy)ethylthio]tetrathiafulvalene

Guidance literature:

With triethyl phosphite; at 120 ℃; for 5h;

DOI:10.1055/s-2000-8203

upstream raw materials:

4,5-bis[(2'-hydroxyethyl)thio]1,3-dithiole-2-thione

tert-butylchlorodiphenylsilane

Downstream raw materials:

4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

4,4',5,5'-tetrakis<2-(tert-butyldiphenylsilyloxy)ethylthio>tetrathiafulvalene

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