tert-butyl 3-(prop-2-ynyl)phenylcarbamate

Base Information

Chemical Name:tert-butyl 3-(prop-2-ynyl)phenylcarbamate
CAS No.:1263482-33-2
Molecular Formula:C₁₄H₁₇NO₂
Molecular Weight:231.294
Hs Code.:

Synonyms:tert-butyl 3-(prop-2-ynyl)phenylcarbamate

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Chemical Property of tert-butyl 3-(prop-2-ynyl)phenylcarbamate

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Technology Process of tert-butyl 3-(prop-2-ynyl)phenylcarbamate

There total 7 articles about tert-butyl 3-(prop-2-ynyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1263482-38-7
tert-butyl 3-(3-(trimethylsilyl)prop-2-ynyl)phenylcarbamate

: 1263482-33-2
tert-butyl 3-(prop-2-ynyl)phenylcarbamate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -20 ℃; for 1h;
DOI:10.1002/cbic.201000422

Reference yield:

: 1367368-47-5
trimethyl(3-(3-nitrophenyl)prop-1-ynyl)silane

: 1263482-33-2
tert-butyl 3-(prop-2-ynyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: tin(ll) chloride / dichloromethane; methanol / 48 h / 20 °C

2: potassium carbonate / tetrahydrofuran; water / 72 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 1.5 h / -20 °C

With tetrabutyl ammonium fluoride; potassium carbonate; tin(ll) chloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/acsmedchemlett.9b00351

Reference yield:

: 3-(3-(trimethylsilyl)prop-2-ynyl)aniline

: 1263482-33-2
tert-butyl 3-(prop-2-ynyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; water / 72 h / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 1.5 h / -20 °C

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; water;
DOI:10.1021/acsmedchemlett.9b00351