Technology Process of C26H25N
There total 5 articles about C26H25N which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Methyltriphenylphosphonium bromide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
C25H23NO;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1039/c4cc01637h
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C
1.2: 20 °C
2.1: trichlorophosphate / 0 - 20 °C / Inert atmosphere
3.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C
3.2: 20 °C
4.1: trichlorophosphate / 0 - 20 °C / Inert atmosphere
5.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C
5.2: 20 °C
With
potassium tert-butylate; trichlorophosphate;
In
tetrahydrofuran;
1.1: |Wittig Olefination / 1.2: |Wittig Olefination / 2.1: |Vilsmeier Reaction / 3.1: |Wittig Olefination / 3.2: |Wittig Olefination / 4.1: |Vilsmeier Reaction / 5.1: |Wittig Olefination / 5.2: |Wittig Olefination;
DOI:10.1039/c4cc01637h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trichlorophosphate / 0 - 20 °C / Inert atmosphere
2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C
2.2: 20 °C
3.1: trichlorophosphate / 0 - 20 °C / Inert atmosphere
4.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C
4.2: 20 °C
With
potassium tert-butylate; trichlorophosphate;
In
tetrahydrofuran;
1.1: |Vilsmeier Reaction / 2.1: |Wittig Olefination / 2.2: |Wittig Olefination / 3.1: |Vilsmeier Reaction / 4.1: |Wittig Olefination / 4.2: |Wittig Olefination;
DOI:10.1039/c4cc01637h
