S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

Base Information

Chemical Name:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide
CAS No.:1147095-69-9
Molecular Formula:C₂₁H₁₇Cl₂N₅O₄S
Molecular Weight:506.369
Hs Code.:

Synonyms:S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

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Chemical Property of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

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Technology Process of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

There total 11 articles about S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1147095-68-8
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-cyano sulfoximide

: 1147095-69-9
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

Guidance literature:: With sulfuric acid; at 5 - 30 ℃; for 3h;

Reference yield:

: 1147096-51-2
methyl 4-[imino(methyl)oxo-λ⁶-sulfanyl]benzoate

: 1147095-69-9
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dichloromethane / 3 h / 15 - 30 °C / Inert atmosphere

2.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 25 - 30 °C

2.2: 0 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

4.1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

5.1: sulfuric acid / 0 - 5 °C

6.1: dmap / dichloromethane / 18 h / 25 - 30 °C

7.1: sulfuric acid / 3 h / 5 - 30 °C

With pyridine; dmap; oxalyl dichloride; sulfuric acid; water; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 114129-35-0
methyl 4-(methylsulfinyl)benzoate

: 1147095-69-9
S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-carbamoyl sulfoximide

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium azide; sulfuric acid / chloroform / 15 h / -20 - 50 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 3 h / 15 - 30 °C / Inert atmosphere

3.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 25 - 30 °C

3.2: 0 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 10 - 30 °C / Inert atmosphere

5.1: tetrahydrofuran / 12 h / 10 - 30 °C / Inert atmosphere

6.1: sulfuric acid / 0 - 5 °C

7.1: dmap / dichloromethane / 18 h / 25 - 30 °C

8.1: sulfuric acid / 3 h / 5 - 30 °C

With pyridine; dmap; sodium azide; oxalyl dichloride; sulfuric acid; water; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; chloroform;