phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

Base Information

Chemical Name:phenyl (S)-1-(2-phenylethyl)-3-butenyl ether
CAS No.:887195-32-6
Molecular Formula:C₁₈H₂₀O
Molecular Weight:252.356
Hs Code.:

Synonyms:phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

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Chemical Property of phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

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Technology Process of phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

There total 2 articles about phenyl (S)-1-(2-phenylethyl)-3-butenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 60340-28-5,98088-55-2,98088-54-1
(R)-1-phenyl-hex-5-en-3-ol

: 108-95-2,27073-41-2
phenol

: 887195-32-6
phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 20 ℃;
DOI:10.3987/COM-05-10652

Reference yield:

: 60340-28-5
1-phenylhex-5-en-3-ol

: 887195-32-6
phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / Amano PS / hexane / 29 h / 20 °C

2: 76 percent / diisopropyl azodicarboxylate; triphenylphosphine / toluene / 20 °C

With Amano PS; di-isopropyl azodicarboxylate; triphenylphosphine; In hexane; toluene;
DOI:10.3987/COM-05-10652

Reference yield: 85.0%

: 887195-32-6
phenyl (S)-1-(2-phenylethyl)-3-butenyl ether

: (S)-3-phenoxy-5-phenylpentanoic acid

Guidance literature:: phenyl (S)-1-(2-phenylethyl)-3-butenyl ether; With potassium permanganate; sodium periodate; potassium carbonate; triphenylphosphine; In water; tert-butyl alcohol; at 20 ℃; for 0.25h;

With ethylene glycol; In water; tert-butyl alcohol; at 20 ℃; for 3h;
DOI:10.3987/COM-05-10652