Tc(SC₆H₄NH)3

Base Information

Chemical Name:Tc(SC₆H₄NH)3
CAS No.:84943-85-1
Molecular Formula:C₁₈H₁₅N₃S₃Tc
Molecular Weight:467.442
Hs Code.:

Synonyms:Tc(SC₆H₄NH)3

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Chemical Property of Tc(SC₆H₄NH)3

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Technology Process of Tc(SC₆H₄NH)3

There total 2 articles about Tc(SC₆H₄NH)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34035-97-7
ammonium pertechnetate

: 137-07-5
2-amino-benzenethiol

: 84943-85-1
Tc(SC₆H₄NH)3

Guidance literature:: With hydrogenchloride; In hydrogenchloride; addn. of NH4TcO4 to excess of ligand in 0.1 N HCl (pptn.); washing (0.1 N HCl), dissoln. in CH2Cl2, drying (Na2SO4), standing (overnight), partial evapn., pptn. on cyclohexane addn.; elem. anal.;
DOI:10.1016/S0020-1693(00)80164-4

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 23288-61-1
pertechnetate anion

: (x)C₆H₅NS^(2-)*(x)Cl^(1-)*(x)Tc⁽³⁺⁾

: tris(2-amidobenzenethiolato^(2-)-S,N)technetate(V)

: 84943-85-1
tris(2-amidobenzenethiolato^(2-)-S,N)technetium(VI)

Guidance literature:: With hydrogen cation; In water; 5 moles of 2-aminobenzenethiol, acidic aq. soln.; main product (brown Tc(V) complex) contaminated by the other two complexes; TLC (Silufol, acetone) and high voltage electrophoresis for detection of contaminants;
DOI:10.1016/S0020-1693(00)90108-7