4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate

Base Information

Chemical Name:4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate
CAS No.:1337933-89-7
Molecular Formula:C₃₈H₃₀N₂O₆
Molecular Weight:610.666
Hs Code.:

Synonyms:4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate

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Technology Process of 4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate

There total 2 articles about 4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 591-50-4
iodobenzene

: 201230-82-2
carbon monoxide

: 130517-95-2,54089-45-1
piperonal N-benzylimine

: 1337933-89-7
4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; In acetonitrile; at 55 ℃; under 3040.2 Torr; Inert atmosphere; sealed glass reaction tube;
DOI:10.1002/anie.201103885

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 100-46-9
benzylamine

: 1337933-89-7
4,5-bis(benzo[d][1,3]dioxol-5-yl)-1,3-dibenzyl-2-phenyl-4,5-dihydro-1H-imidazol-3-ium-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chloride / water / Inert atmosphere

2: bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine / acetonitrile / 55 °C / 3040.2 Torr / Inert atmosphere; sealed glass reaction tube

With bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; sodium chloride; In water; acetonitrile;
DOI:10.1002/anie.201103885