4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

Base Information

Chemical Name:4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate
CAS No.:1035596-23-6
Molecular Formula:C₁₆H₁₀FN₃O₅S₃
Molecular Weight:439.469
Hs Code.:

Synonyms:4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

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Chemical Property of 4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

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Technology Process of 4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

There total 4 articles about 4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18274-81-2
desmethyl anethole trithione

: 70767-70-3
2-(5-fluorouracil-1-carboxamide)acetic acid

: 1035596-23-6
4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield:

: 532-11-6
anethole trithione

: 1035596-23-6
4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / 0.42 h / 215 °C

2: dicyclohexyl-carbodiimide / dmap / tetrahydrofuran / 0.5 h / 20 °C

With pyridine hydrochloride; dicyclohexyl-carbodiimide; dmap; In tetrahydrofuran;

Reference yield:

: 1035596-25-8
2-(5-fluorouracil-1-carboxamide)ethyl acetate

: 1035596-23-6
4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(5-fluoro-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-1-carboxamido)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / 0.5 h / 70 °C

2: dicyclohexyl-carbodiimide / dmap / tetrahydrofuran / 0.5 h / 20 °C

With hydrogenchloride; water; dicyclohexyl-carbodiimide; dmap; In tetrahydrofuran;