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Technology Process of In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

Base Information
  • Chemical Name:In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8
  • CAS No.:1259035-45-4
  • Molecular Formula:C42H56BF2N8O8*In
  • Molecular Weight:964.583
  • Hs Code.:
In<sup>(3+)</sup>*((C<sub>8</sub>H<sub>16</sub>N<sub>4</sub>)(CH<sub>2</sub>C(O)O)3)CH<sub>2</sub>C(O)NHCH<sub>2</sub>CH<sub>2</sub>NHC(O)(C<sub>6</sub>H<sub>4</sub>)((C<sub>9</sub>BN<sub>2</sub>)(F)2(CH<sub>3</sub>)4(CH<sub>2</sub>CH<sub>3</sub>)2)<sup>(3-)</sup>=C<sub>42</sub>H<sub>56</sub>BF<sub>2</sub>InN<sub>8</sub>O<sub>8</sub>

Synonyms:In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

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Chemical Property of In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8
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Technology Process of In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

There total 3 articles about In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

((C<sub>8</sub>H<sub>16</sub>N<sub>4</sub>)(CH<sub>2</sub>C(O)OH)3)CH<sub>2</sub>C(O)NHCH<sub>2</sub>CH<sub>2</sub>NHC(O)(C<sub>6</sub>H<sub>4</sub>)((C<sub>9</sub>BN<sub>2</sub>)(F)2(CH<sub>3</sub>)4(CH<sub>2</sub>CH<sub>3</sub>)2)

((C8H16N4)(CH2C(O)OH)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)

indium(III) chloride
10025-82-8

indium(III) chloride

In<sup>(3+)</sup>*((C<sub>8</sub>H<sub>16</sub>N<sub>4</sub>)(CH<sub>2</sub>C(O)O)3)CH<sub>2</sub>C(O)NHCH<sub>2</sub>CH<sub>2</sub>NHC(O)(C<sub>6</sub>H<sub>4</sub>)((C<sub>9</sub>BN<sub>2</sub>)(F)2(CH<sub>3</sub>)4(CH<sub>2</sub>CH<sub>3</sub>)2)<sup>(3-)</sup>=C<sub>42</sub>H<sub>56</sub>BF<sub>2</sub>InN<sub>8</sub>O<sub>8</sub>
1259035-45-4

In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

Guidance literature:
In ethanol; water; react. 1 equiv. of InCl3 with ligand at 35°C in aq. EtOH for 2 h;
DOI:10.1039/c0cc02749a

Reference yield:

4,4-difluoro-8-(4-((succinimid-N-yl)oxycarbonyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene
1218921-99-3

4,4-difluoro-8-(4-((succinimid-N-yl)oxycarbonyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene

In<sup>(3+)</sup>*((C<sub>8</sub>H<sub>16</sub>N<sub>4</sub>)(CH<sub>2</sub>C(O)O)3)CH<sub>2</sub>C(O)NHCH<sub>2</sub>CH<sub>2</sub>NHC(O)(C<sub>6</sub>H<sub>4</sub>)((C<sub>9</sub>BN<sub>2</sub>)(F)2(CH<sub>3</sub>)4(CH<sub>2</sub>CH<sub>3</sub>)2)<sup>(3-)</sup>=C<sub>42</sub>H<sub>56</sub>BF<sub>2</sub>InN<sub>8</sub>O<sub>8</sub>
1259035-45-4

In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

Guidance literature:
Multi-step reaction with 2 steps
1: water; acetonitrile
2: water; ethanol
In ethanol; water; acetonitrile;
DOI:10.1039/c0cc02749a

Reference yield:

2,2',2''-(10-(2-((2-aminoethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid

2,2',2''-(10-(2-((2-aminoethyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetic acid

In<sup>(3+)</sup>*((C<sub>8</sub>H<sub>16</sub>N<sub>4</sub>)(CH<sub>2</sub>C(O)O)3)CH<sub>2</sub>C(O)NHCH<sub>2</sub>CH<sub>2</sub>NHC(O)(C<sub>6</sub>H<sub>4</sub>)((C<sub>9</sub>BN<sub>2</sub>)(F)2(CH<sub>3</sub>)4(CH<sub>2</sub>CH<sub>3</sub>)2)<sup>(3-)</sup>=C<sub>42</sub>H<sub>56</sub>BF<sub>2</sub>InN<sub>8</sub>O<sub>8</sub>
1259035-45-4

In(3+)*((C8H16N4)(CH2C(O)O)3)CH2C(O)NHCH2CH2NHC(O)(C6H4)((C9BN2)(F)2(CH3)4(CH2CH3)2)(3-)=C42H56BF2InN8O8

Guidance literature:
Multi-step reaction with 2 steps
1: water; acetonitrile
2: water; ethanol
In ethanol; water; acetonitrile;
DOI:10.1039/c0cc02749a
upstream raw materials:

indium(III) chloride

4,4-difluoro-8-(4-((succinimid-N-yl)oxycarbonyl)phenyl)-1,3,5,7-tetramethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene

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