Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester

Base Information

• Chemical Name: Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester
• CAS No.: 1220982-49-9
• Molecular Formula: C₃₅H₃₆NO₇P
• Molecular Weight: 613.647

Synonyms:Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester

Chemical Property of Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester

Chemical Property:

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Technology Process of Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester

There total 1 articles about Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methylphosphonic chloride isopropyl ester (1445-76-7) + 2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-(4-hydroxyphenyl)propionic acid benzyl ester (82911-77-1) → Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester (1220982-49-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0030-1258132

Reference yield: 85.0%

Fmoc-tyrosine(O-isopropyl methylphosphonate) benzyl ester (1220982-49-9) → Fmoc-tyrosine(O-isopropyl methylphosphonate) (1220982-57-9)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; for 2h;

DOI:10.1055/s-0030-1258132

upstream raw materials:

methylphosphonic chloride isopropyl ester

2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-(4-hydroxyphenyl)propionic acid benzyl ester

Downstream raw materials:

Fmoc-tyrosine(O-isopropyl methylphosphonate)

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