C₂₉H₃₈O₄Si

Base Information

• Chemical Name: C₂₉H₃₈O₄Si
• CAS No.: 1334173-54-4
• Molecular Formula: C₂₉H₃₈O₄Si
• Molecular Weight: 478.704
• Mol file: 1334173-54-4.mol

Synonyms:C₂₉H₃₈O₄Si

Chemical Property of C₂₉H₃₈O₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₈O₄Si

There total 6 articles about C₂₉H₃₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H42O4Si2 (1334173-62-4) → C29H38O4Si (1334173-54-4)

Guidance literature:

With hydrogenchloride; In methanol; water; at 0 ℃; for 1h;

DOI:10.1002/anie.201103550

Reference yield:

C25H30O3Si (1334173-57-7) → C29H38O4Si (1334173-54-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

1.2: 13 h / -78 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: dicobalt octacarbonyl / toluene / 1.5 h / 20 °C / Inert atmosphere

3.2: 12 h / 100 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; dicobalt octacarbonyl; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 3.1: Pauson-Khand reaction / 3.2: Pauson-Khand reaction;

DOI:10.1002/anie.201103550

Reference yield:

C26H34O4Si → C29H38O4Si (1334173-54-4)

Guidance literature:

Multi-step reaction with 4 steps

1.1: pyridinium p-toluenesulfonate / isopropyl alcohol; toluene / 28 - 80 °C / Inert atmosphere

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2.2: 13 h / -78 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: dicobalt octacarbonyl / toluene / 1.5 h / 20 °C / Inert atmosphere

4.2: 12 h / 100 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; dicobalt octacarbonyl; pyridinium p-toluenesulfonate; lithium hexamethyldisilazane; In tetrahydrofuran; isopropyl alcohol; toluene; 4.1: Pauson-Khand reaction / 4.2: Pauson-Khand reaction;

DOI:10.1002/anie.201103550

upstream raw materials:

C₂₈H₃₄O₃Si

C₂₈H₃₈O₃Si

C₃₁H₄₂O₄Si₂

C₂₅H₃₀O₃Si

Downstream raw materials:

C₃₃H₄₈O₆Si

C₄₁H₅₆O₇SSi

C₃₅H₅₀O₆Si

C₃₆H₅₂O₅Si