Technology Process of C71H81N7O14
There total 3 articles about C71H81N7O14 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C45H57N8O9Pol;
With
trimethylphosphane;
In
tetrahydrofuran; water; toluene;
for 1h;
2-chlorotrityl resin
Inert atmosphere;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 0.0166667h;
2-chlorotrityl resin
Inert atmosphere;
(S)-4-(2-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)benzoic acid;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere
2.1: trimethylphosphane / tetrahydrofuran; toluene; water / 1 h / Inert atmosphere
2.2: 0.02 h / 20 °C / Inert atmosphere
2.3: Inert atmosphere
With
trifluoroacetic acid; trimethylphosphane;
In
tetrahydrofuran; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere
3.1: trimethylphosphane / tetrahydrofuran; toluene; water / 1 h / Inert atmosphere
3.2: 0.02 h / 20 °C / Inert atmosphere
3.3: Inert atmosphere
With
4-methyl-morpholine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; trimethylphosphane;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;