6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

Base Information

Chemical Name:6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole
CAS No.:512779-66-7
Molecular Formula:C₂₅H₂₃NO₃S₂
Molecular Weight:449.595
Hs Code.:

6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1<i>H</i>-carbazole

Synonyms:6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

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Chemical Property of 6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

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Technology Process of 6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

There total 5 articles about 6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 4922-47-8
1-(phenylthio)cyclohex-1-ene

: 512779-50-9
N-(4-benzenesulfinyl-phenyl)-4-methyl-benzenesulfonamide

: 512779-66-7
6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

Guidance literature:: 1-(phenylthio)cyclohex-1-ene; N-(4-benzenesulfinyl-phenyl)-4-methyl-benzenesulfonamide; With trifluoroacetic anhydride; In acetonitrile; at 0 ℃;

With 3-chloro-benzenecarboperoxoic acid;

Reference yield:

: 1135-14-4
4-aminophenyl phenyl sulfide

: 512779-66-7
6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; DMAP / CH₂Cl₂

2.1: mCPBA / CH₂Cl₂ / -40 °C

3.1: (CF₃CO)2O / acetonitrile / 0 °C

3.2: 57 percent / mCPBA

With pyridine; dmap; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane; acetonitrile;

Reference yield:

: 51170-34-4
4'-Phenylthio-4-toluolsulfanilid

: 512779-66-7
6-benzenesulfinyl-9-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: mCPBA / CH₂Cl₂ / -40 °C

2.1: (CF₃CO)2O / acetonitrile / 0 °C

2.2: 57 percent / mCPBA

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane; acetonitrile;