2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

Base Information

Chemical Name:2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol
CAS No.:1346168-51-1
Molecular Formula:C₃₆H₂₅N₅O
Molecular Weight:543.627
Hs Code.:

Synonyms:2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

Chemical Property:

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Technology Process of 2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

There total 7 articles about 2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1359296-39-1
C₃₆H₂₅ClN₂O

: 1346168-51-1
2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 70 ℃; for 12h;
DOI:10.1039/c1ob06151h

Reference yield:

: 134-81-6
benzil

: 1346168-51-1
2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 20 - 110 °C

2: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

3: thionyl chloride / dichloromethane / 2 h / 20 °C

4: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C

With copper(l) iodide; thionyl chloride; sodium azide; bis(triphenylphosphine)palladium(II) chloride; triethylamine; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06151h

Reference yield:

: 1346168-55-5
2-(1-(4-iodophenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

: 1346168-51-1
2-(1-(4-((4-(azidomethyl)phenyl)ethynyl)phenyl)-4,5-diphenyl-1H-imidazol-2-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: thionyl chloride / dichloromethane / 2 h / 20 °C

3: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C

With copper(l) iodide; thionyl chloride; sodium azide; bis(triphenylphosphine)palladium(II) chloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06151h