2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

Base Information

Chemical Name:2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane
CAS No.:1072709-45-5
Molecular Formula:C₃₇H₅₂O₅Si
Molecular Weight:604.902
Hs Code.:

Synonyms:2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

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Chemical Property of 2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

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Technology Process of 2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

There total 6 articles about 2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1072709-43-3
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1072709-45-5
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 18 ℃; for 20h;

Reference yield:

: 621-59-0
isovanillin

: 1072709-45-5
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 42 h / 18 °C

2.1: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C

2.2: 0.5 h / -78 °C

2.3: -78 - 18 °C

3.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 18 °C

4.1: sodium hydride / tetrahydrofuran / 0.08 h / 18 °C

4.2: 2.5 h

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 18 °C

6.1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 0 - 18 °C

6.2: 3 h / 0 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 18 °C

With 1H-imidazole; hydrogenchloride; lithium aluminium tetrahydride; N,N,N,N,-tetramethylethylenediamine; water; tert.-butyl lithium; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; pentane;

Reference yield:

: 1072709-37-5
4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexanone

: 1072709-45-5
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]cyclohexyl}ethoxy-tert-butyldiphenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.08 h / 18 °C

1.2: 2.5 h

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 18 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 0 - 18 °C

3.2: 3 h / 0 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 h / 18 °C

With 1H-imidazole; lithium aluminium tetrahydride; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;