2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

Base Information

Chemical Name:2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol
CAS No.:1072709-43-3
Molecular Formula:C₂₁H₃₄O₅
Molecular Weight:366.498
Hs Code.:

Synonyms:2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

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Chemical Property of 2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

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Technology Process of 2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

There total 6 articles about 2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1072709-41-1
ethyl 2-{4-[methoxymethoxy (3-isopropoxy-4-methoxyphenyl)methyl]-cyclohexylidene}acetate

: 1072709-43-3
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

Guidance literature:: ethyl 2-{4-[methoxymethoxy (3-isopropoxy-4-methoxyphenyl)methyl]-cyclohexylidene}acetate; With lithium aluminium tetrahydride; In diethyl ether; at 0 - 18 ℃; for 3.5h;

With hydrogen; 5% rhodium on activated aluminium oxide; In ethyl acetate; at 0 ℃; for 3h;

Reference yield:

: 1072709-37-5
4-[hydroxyl(3-isopropoxy-4-methoxyphenyl)methyl]cyclohexanone

: 1072709-43-3
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.08 h / 18 °C

1.2: 2.5 h

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 18 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 0 - 18 °C

3.2: 3 h / 0 °C

With lithium aluminium tetrahydride; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 621-59-0
isovanillin

: 1072709-43-3
2-{4-[(3-isopropoxy-4-methoxyphenyl)(methoxymethoxy)methyl]-cyclohexyl}ethanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 42 h / 18 °C

2.1: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / diethyl ether; pentane / 0.17 h / -78 °C

2.2: 0.5 h / -78 °C

2.3: -78 - 18 °C

3.1: hydrogenchloride; water / tetrahydrofuran / 24 h / 18 °C

4.1: sodium hydride / tetrahydrofuran / 0.08 h / 18 °C

4.2: 2.5 h

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 18 °C

6.1: lithium aluminium tetrahydride / diethyl ether / 3.5 h / 0 - 18 °C

6.2: 3 h / 0 °C

With hydrogenchloride; lithium aluminium tetrahydride; N,N,N,N,-tetramethylethylenediamine; water; tert.-butyl lithium; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; pentane;