(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine

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Chemical Name:(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine
CAS No.:1225448-64-5
Molecular Formula:C₂₈H₄₉NO₃Si
Molecular Weight:475.787
Hs Code.:

Synonyms:(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine

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Technology Process of (2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine

There total 1 articles about (2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1225448-50-9
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

: [3-(methoxymethoxy)propyl]triphenylphosphonium bromide

: 1225448-64-5
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine

Guidance literature:: [3-(methoxymethoxy)propyl]triphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere;

(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.3987/COM-09-S(S)130