(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

Base Information

Chemical Name:(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde
CAS No.:1225448-50-9
Molecular Formula:C₂₃H₃₉NO₂Si
Molecular Weight:389.654
Hs Code.:

Synonyms:(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

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Technology Process of (2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

There total 1 articles about (2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1225448-48-5
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-hydroxymethyl-2-pentylpyrrolidine

: 1225448-50-9
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.3987/COM-09-S(S)130

Reference yield: 90.0%

: 1225448-50-9
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

: 86608-70-0
2-(1,3-dioxolan-2-yl)ethyl(triphenyl)phosphonium bromide

: 1225448-51-0
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[3-(1,3-dioxolan-2-yl)propenyl]-2-pentylpyrrolidine

Guidance literature:: 2-(1,3-dioxolan-2-yl)ethyl(triphenyl)phosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere;

(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.3987/COM-09-S(S)130

Reference yield: 83.0%

: 1225448-50-9
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde

: [3-(methoxymethoxy)propyl]triphenylphosphonium bromide

: 1225448-64-5
(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-[(4-methoxymethoxy)but-1-enyl]-2-pentylpyrrolidine

Guidance literature:: [3-(methoxymethoxy)propyl]triphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere;

(2S,4R)-4-(tert-butyldimethylsilyloxy)-1-benzyl-2-pentyl-2-pyrrolidinecarboxaldehyde; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.3987/COM-09-S(S)130