N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

Base Information

Chemical Name:N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine
CAS No.:89637-94-5
Molecular Formula:C₅₉H₇₈N₁₄O₁₄
Molecular Weight:1207.35
Hs Code.:

N<sup>α</sup>-(tert-butyloxycarbonyl)-N<sup>ε</sup>-<N-(4-amino-4-deoxy-N<sup>10</sup>-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N<sup>ε</sup>-(benzyloxycarbonyl)-L-lysyl-N<sup>ε</sup>-(benzyloxycarbonyl)-L-lysine

Synonyms:N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

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Chemical Property of N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

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Technology Process of N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

There total 8 articles about N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 89637-93-4
N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine benzyl(α-Glu)methyl(Lys) ester

: 89637-94-5
N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

Guidance literature:: With barium dihydroxide; In ethanol; water; Ambient temperature;
DOI:10.1021/jm00373a014

Reference yield:

: 13030-09-6
1-benzyl L-glutamate

: 89637-94-5
N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / Et₃N / benzene / Ambient temperature

2: 1.) diethyl phosphorocyanidate, Et₃N / 1.) DMF, overnight, RT, 2.) DMF, RT, 3 d

3: Et₃N / dimethylformamide / 0.33 h / Ambient temperature

4: dimethylformamide / Ambient temperature

5: 74 percent / diphenylphosphoryl azide, Et₃N / dimethylformamide / 0 - 20 °C

6: 94 percent / Ba(OH)2*8H₂O / ethanol; H₂O / Ambient temperature

With barium dihydroxide; diethyl cyanophosphonate; diphenylphosphoranyl azide; triethylamine; In ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00373a014

Reference yield:

: 13734-28-6
Boc-Lys-OH

: 89637-94-5
N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / Et₃N / benzene / Ambient temperature

2: dimethylformamide / Ambient temperature

3: 74 percent / diphenylphosphoryl azide, Et₃N / dimethylformamide / 0 - 20 °C

4: 94 percent / Ba(OH)2*8H₂O / ethanol; H₂O / Ambient temperature

With barium dihydroxide; diphenylphosphoranyl azide; triethylamine; In ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00373a014

upstream raw materials:

N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine benzyl(α-Glu)methyl(Lys) ester

1-benzyl L-glutamate

Boc-Lys-OH

C₁₇H₃₈N₂O₄Si₂

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Encyclopedia

Technology Process of N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

NAVIGATION

Encyclopedia

Technology Process of Nα-(tert-butyloxycarbonyl)-Nε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-Nε-(benzyloxycarbonyl)-L-lysyl-Nε-(benzyloxycarbonyl)-L-lysine

Nα-(tert-butyloxycarbonyl)-Nε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-Nε-(benzyloxycarbonyl)-L-lysyl-Nε-(benzyloxycarbonyl)-L-lysine

NAVIGATION

Technology Process of N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine

N^α-(tert-butyloxycarbonyl)-N^ε-10-methylpteroyl)-L-γ-glutamyl>-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine