tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Base Information

Chemical Name:tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate
CAS No.:1345893-80-2
Molecular Formula:C₂₄H₃₀BrNO₃
Molecular Weight:460.411
Hs Code.:

Synonyms:tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Suppliers and Price of tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

There total 3 articles about tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1345893-78-8
tert-butyl but-3-enyl(R)-1-phenylethylcarbamate

: 7154-66-7
2-bromobenzoic acid chloride

: 1345893-80-2
tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Guidance literature:: tert-butyl but-3-enyl(R)-1-phenylethylcarbamate; With Schwartz's reagent; In dichloromethane; Inert atmosphere;

2-bromobenzoic acid chloride; With copper(I) bromide dimethylsulfide complex; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol202796w

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1345893-80-2
tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane / Inert atmosphere

2.1: Schwartz's reagent / dichloromethane / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With dmap; Schwartz's reagent; triethylamine; In dichloromethane;
DOI:10.1021/ol202796w

Reference yield:

: 177944-16-0
(R)-N-(but-3-en-1-yl)-N-(α-methylbenzyl)amine

: 1345893-80-2
tert-butyl 5-(2-bromophenyl)-5-oxophenylpentyl-(R)-1-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane / Inert atmosphere

2.1: Schwartz's reagent / dichloromethane / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With dmap; Schwartz's reagent; triethylamine; In dichloromethane;
DOI:10.1021/ol202796w