diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

Base Information

Chemical Name:diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate
CAS No.:1173188-97-0
Molecular Formula:C₂₀H₂₀ClNO₆S
Molecular Weight:437.901
Hs Code.:

Synonyms:diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

Chemical Property:

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Technology Process of diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

There total 4 articles about diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 13707-45-4
N-benzylidene-4-chlorobenzenesulfonamide

: 105-53-3
diethyl malonate

: 1173188-97-0
diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

Guidance literature:: With iodosylbenzene; potassium iodide; In acetonitrile; at 25 ℃;
DOI:10.1016/j.tetlet.2009.04.056

Reference yield:

: 13707-45-4
N-benzylidene-4-chlorobenzenesulfonamide

: 685-87-0
Diethyl 2-bromomalonate

: 1173188-97-0
diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

Guidance literature:: With sodium hydride; In acetonitrile; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2019.151576

Reference yield:

: 98-64-6
4-Chlorobenzenesulfonamide

: 1173188-97-0
diethyl 1-((4-chlorophenyl)sulfonyl)-3-phenylaziridine-2,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: pyrrolidine / dichloromethane / 20 h / 60 °C / Inert atmosphere; Molecular sieve; Schlenk technique

2: sodium hydride / mineral oil; acetonitrile / 0 - 20 °C / Inert atmosphere

With pyrrolidine; sodium hydride; In dichloromethane; acetonitrile; mineral oil;
DOI:10.1016/j.tetlet.2019.151576