2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde

Base Information

Chemical Name:2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde
CAS No.:182067-54-5
Molecular Formula:C9H9 N O5
Molecular Weight:211.17146
Hs Code.:
DSSTox Substance ID:DTXSID60444022
Wikidata:Q82262024
Mol file:182067-54-5.mol

Synonyms:2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde;182067-54-5;Benzaldehyde, 2-ethoxy-3-hydroxy-4-nitro- (9CI);DTXSID60444022

Suppliers and Price of 2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde

Chemical Property:

PSA：92.35000
LogP:2.03480
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:211.04807239
Heavy Atom Count:15
Complexity:239

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=C(C=CC(=C1O)[N+](=O)[O-])C=O

Technology Process of 2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde

There total 2 articles about 2-Ethoxy-3-hydroxy-4-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 182067-51-2
2-ethoxy-3-hydroxybenzaldehyde

: 2,3-dihydroxy-6-nitrobenzaldehyde

: 182067-57-8
2-ethoxy-3-hydroxy-6-nitrobenzaldehyde

: 182067-54-5
2-ethoxy-3-hydroxy-4-nitrobenzaldehyde

Guidance literature:: With nitric acid; acetic acid; In toluene; at 5 - 10 ℃; for 0.0833333h;
DOI:10.1248/cpb.44.1484

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 182067-54-5
2-ethoxy-3-hydroxy-4-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH, DMSO / 1.) 110 deg C, 2 h, 2.) RT, 18 h

2: 22 percent / 70percent aq. HNO₃, AcOH / toluene / 0.08 h / 5 - 10 °C

With nitric acid; sodium hydride; acetic acid; dimethyl sulfoxide; In toluene;
DOI:10.1248/cpb.44.1484