4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

Base Information

Chemical Name:4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine
CAS No.:74177-56-3
Molecular Formula:C₁₄H₈F₁₂N₂O₂
Molecular Weight:464.211
Hs Code.:

Synonyms:4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

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Chemical Property of 4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

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Technology Process of 4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

There total 1 articles about 4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 684-16-2
Hexafluoroacetone

: 22265-37-8
4-methoxybenzamidine

: 74177-56-3
4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

Guidance literature:: With pyridine; trichlorophosphate; In diethyl ether; at -15 ℃; for 72h;
DOI:10.1016/S0022-1139(00)85154-4

Reference yield: 100.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 74177-56-3
4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

: 4-(4-Methoxy-phenyl)-3-methyl-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

Guidance literature:: In diethyl ether; Ambient temperature;
DOI:10.1016/S0022-1139(00)85154-4

Reference yield:

: 74177-56-3
4-(4-Methoxy-phenyl)-2,2,6,6-tetrakis-trifluoromethyl-3,6-dihydro-2H-[1,3,5]oxadiazine

: C₃₆H₃₀F₁₈N₆O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / diethyl ether / Ambient temperature

2: 180 - 200 °C / 80 Torr

In diethyl ether;
DOI:10.1016/S0022-1139(00)85154-4