methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside

Base Information

• Chemical Name: methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside
• CAS No.: 1261355-77-4
• Molecular Formula: C₄₇H₆₃O₁₉S*Na
• Molecular Weight: 987.062

Synonyms:methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside

Chemical Property of methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside

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Technology Process of methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside

There total 27 articles about methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside (1393472-09-7) → methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside (1261355-77-4)

Guidance literature:

With sodium iodide; In acetone; at 20 ℃; for 12h;

DOI:10.1016/j.tet.2012.06.081

Reference yield: 82.0%

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside (1261355-75-2) + methyl iodide (74-88-4) → methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside (1261355-77-4)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2010.10.042

Reference yield: 49.0%

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl b-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methylsulfonatomethyl)-α-D-glucopyranoside (1261355-91-2) + methyl iodide (74-88-4) → methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(sodium sulfonatomethyl)-α-D-glucopyranoside (1261355-77-4)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/j.tetlet.2010.10.042

upstream raw materials:

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl 3-O-methyl-β-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methyl sulfonatomethyl)-α-D-glucopyranoside

methyl iodide

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-(methyl b-D-glucopyranosyluronate)-(1->4)-2,6-di-O-benzyl-3-deoxy-3-C-(methylsulfonatomethyl)-α-D-glucopyranoside

methyl (6-O-benzyl-2,3,4-tri-O-methyl-α-D-glucopyranosyl)-(1->4)-2-O-acetyl-3-O-methyl-1-O-trichloroacetimidoyl-D-glucopyranosyluronate

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