tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

Base Information

Chemical Name:tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride
CAS No.:1365803-25-3
Molecular Formula:C₁₇H₂₆F₃N₃O₂*ClH
Molecular Weight:397.868
Hs Code.:

Synonyms:tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

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Chemical Property of tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

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Technology Process of tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

There total 5 articles about tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1365803-24-2
tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate

: 1365803-25-3
tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; diethyl ether; at 20 ℃; for 1h;

Reference yield:

: 401-94-5
3-nitro-5-(trifluoromethyl)-phenylamine

: 1365803-25-3
tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; triethylamine / dichloromethane / 15 h / 0 °C

2: caesium carbonate / acetonitrile / 4 h / 100 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 3102.97 Torr

4: hydrogenchloride / diethyl ether; methanol / 1 h / 20 °C

With hydrogenchloride; dmap; hydrogen; caesium carbonate; triethylamine; palladium 10% on activated carbon; In methanol; diethyl ether; dichloromethane; acetonitrile;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1365803-25-3
tert-butyl [3-amino-5-(trifluoromethyl)phenyl][3-(dimethylamino)propyl]carbamate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; triethylamine / dichloromethane / 15 h / 0 °C

2: caesium carbonate / acetonitrile / 4 h / 100 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 3102.97 Torr

4: hydrogenchloride / diethyl ether; methanol / 1 h / 20 °C

With hydrogenchloride; dmap; hydrogen; caesium carbonate; triethylamine; palladium 10% on activated carbon; In methanol; diethyl ether; dichloromethane; acetonitrile;