1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

Base Information

Chemical Name:1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene
CAS No.:691881-31-9
Molecular Formula:C₂₀H₂₆N₂OS
Molecular Weight:342.505
Hs Code.:

Synonyms:1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

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Chemical Property of 1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

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Technology Process of 1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

There total 4 articles about 1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 691881-30-8
3-cyclohexyl-1-(2-hydroxy-2-methylpropyl)-4-(4-methylthiophenyl)pyrazol-5-ol

: 691881-31-9
1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

Guidance literature:: With phosphoric acid; at 70 ℃; for 6h;
DOI:10.1016/j.bmc.2004.01.012

Reference yield:

: 16188-55-9
2-(4-(methylthio)phenyl)acetic acid

: 691881-31-9
1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / H₂SO₄ / 16 h / 50 °C

2.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 1.17 h / -78 - 20 °C

2.2: 99 percent / tetrahydrofuran / 2 h / -78 - 0 °C

3.1: 68 percent / glacial AcOH / 5 h / 95 °C

4.1: 33 percent / phosphoric acid / 6 h / 70 °C

With phosphoric acid; sulfuric acid; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/j.bmc.2004.01.012

Reference yield:

: 70290-37-8
(4-methylsulfanyl-phenyl)-acetic acid methyl ester

: 691881-31-9
1-(6-cyclohexyl-2,2-dimethyl(3H-pyrazolo[5,1-b]1,3-oxazolidin-7-yl))-4-methylthiobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 1.17 h / -78 - 20 °C

1.2: 99 percent / tetrahydrofuran / 2 h / -78 - 0 °C

2.1: 68 percent / glacial AcOH / 5 h / 95 °C

3.1: 33 percent / phosphoric acid / 6 h / 70 °C

With phosphoric acid; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/j.bmc.2004.01.012