tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

Base Information

Chemical Name:tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate
CAS No.:1010136-50-1
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:305.374
Hs Code.:

Synonyms:tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

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Chemical Property of tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

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Technology Process of tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

There total 12 articles about tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: tert-butyl {(1S,2S)-1-hydroxy-1-[(R)-2-methyloxiran-2-yl]-3-phenylpropan-2-yl}carbamate

: 1010136-50-1,1416709-77-7
tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

Guidance literature:: With sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; Green chemistry;
DOI:10.3184/174751916X14539789662063

Reference yield: 54.0%

: (2S)-N-(4-methyl-3-oxo-1-phenylpent-4-en-2-yl)carbamic acid tert-butyl ester

: 1010136-50-1,1416709-77-7
tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

: 1416709-77-7
[(S)-1-benzyl-2-((S)-2-methyloxiranyl)-2-oxo-ethyl]carbamic acid tert-butyl ester

Guidance literature:: With dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; In methanol; water; benzonitrile; at 0 - 20 ℃;

Reference yield: 32.0%

: (2S)-N-(4-methyl-3-oxo-1-phenylpent-4-en-2-yl)carbamic acid tert-butyl ester

: 1010136-50-1,1416709-77-7
tert-butyl [(1S)-1-[(2R)-2-methyloxiran-2-yl]-1-oxo-3-phenylpropan-2-yl]carbamate

Guidance literature:: With dihydrogen peroxide; benzonitrile; N-ethyl-N,N-diisopropylamine; In methanol; at 0 ℃;
DOI:10.1021/acs.jmedchem.0c00416