C₃₃H₃₁F₆N₃O₆

Base Information

Chemical Name:C₃₃H₃₁F₆N₃O₆
CAS No.:1195951-73-5
Molecular Formula:C₃₃H₃₁F₆N₃O₆
Molecular Weight:679.616
Hs Code.:

C<sub>33</sub>H<sub>31</sub>F<sub>6</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₃₃H₃₁F₆N₃O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₁F₆N₃O₆

Chemical Property:

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Technology Process of C₃₃H₃₁F₆N₃O₆

There total 9 articles about C₃₃H₃₁F₆N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1195951-72-4
C₂₆H₁₈F₆N₂O₅

: 58620-93-2
tert-butyl 3-aminopropanoate hydrochloride

: 1195951-73-5
C₃₃H₃₁F₆N₃O₆

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 72h;

Reference yield:

: 852471-18-2
3-benzyloxy-4-(4-trifluoromethoxyphenyl)-1H-pyrazole

: 1195951-73-5
C₃₃H₃₁F₆N₃O₆

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine; copper diacetate / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve

2: hydrogen / 10 percent palladium on barium sulphate / methanol / 18 h / 25 °C / 760.05 Torr

3: pyridine; copper diacetate / dichloromethane / Molecular sieve

4: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

5: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 72 h / 20 °C

With pyridine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; copper diacetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; 10 percent palladium on barium sulphate; In methanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 95299-18-6
methyl 2-(4-(trifluoromethoxy)phenyl)acetate

: 1195951-73-5
C₃₃H₃₁F₆N₃O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 20 °C

2.1: hydrazine hydrate / ethanol / 48 h / 20 °C

3.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C

3.2: 0.17 h / 20 °C

4.1: pyridine; copper diacetate / 1,2-dichloro-ethane / 48 h / 20 °C / Molecular sieve

5.1: hydrogen / 10 percent palladium on barium sulphate / methanol / 18 h / 25 °C / 760.05 Torr

6.1: pyridine; copper diacetate / dichloromethane / Molecular sieve

7.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / acetonitrile / 72 h / 20 °C

With pyridine; di-tert-butyl-diazodicarboxylate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; copper diacetate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; 10 percent palladium on barium sulphate; In tetrahydrofuran; methanol; ethanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;